Jun 14, 2022 · EPA Method 8260D (SW-846): Volatile Organic Compounds by Gas Chromatography-Mass Spectrometry (GC/MS) This document is included in Selected Analytical Methods for Environmental Remediation and Recovery (SAM) . Citation: U.S. EPA. 2006. "Method 8260D (SW-846): Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS)," Revision 3.